N-Hydroxyphthalimide → HCID 25137666, compound

HRID 1663121Notes

Reaction equation

HRID 1663121 reaction equation
O[N:2]1C(=O)C2=CC=CC=C2C1=O.[OH:13][CH2:14][CH2:15][C:16]1[CH:23]=[CH:22][C:19]([C:20]#[N:21])=[CH:18][CH:17]=1>>[NH2:2][O:13][CH2:14][CH2:15][C:16]1[CH:23]=[CH:22][C:19]([C:20]#[N:21])=[CH:18][CH:17]=1

Participants

3

Reactant 2

HCID 10665N-HydroxyphthalimideHCID 28008154-(2-Hydroxyethyl)benzonitrile

Product 1

HCID 25137666HCID 25137666, compound

Procedure

Prepared by a similar procedure as described for preparation 31. Starting materials: N-hydroxyphthalimide and 4-(2-hydroxyethyl)benzonitrile (Maybridge). 13C-NMR (DMSO-d6) δ 145.6, 131.9, 129.9, 118.9, 108.7, 74.6, 34.3.

Workup

  1. customPrepared by a similar procedure
  2. customas described for preparation 31

Sources & evidence

ORD record
ord-8d6f049ebfce4e44a75c91db4ef5e232
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

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