N-Hydroxyphthalimide → O-Cyclooctylmethyl-hydroxylamine

HRID 1663124Notes

Reaction equation

HRID 1663124 reaction equation
O[N:2]1C(=O)C2=CC=CC=C2C1=O.[CH:13]1([CH2:21][OH:22])[CH2:20][CH2:19][CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1>>[CH:13]1([CH2:21][O:22][NH2:2])[CH2:20][CH2:19][CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1

Participants

3

Reactant 2

HCID 10665N-HydroxyphthalimideHCID 77196Cyclooctanemethanol

Product 1

HCID 58989793O-Cyclooctylmethyl-hydroxylamine

Procedure

Prepared by a similar procedure as described for preparation 31. Starting materials: N-hydroxyphthalimide and cyclooctanemethanol (Acros). 13C-NMR (CDCl3) δ 82.3, 36.4, 29.4, 27.0, 26.5, 25.5.

Workup

  1. customPrepared by a similar procedure
  2. customas described for preparation 31

Sources & evidence

ORD record
ord-751f189bf9854de2a54d4469b9b0446b
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

Loading…