N-Hydroxyphthalimide → O-(3-cyclopentylpropyl)hydroxylamine

HRID 1663126Notes

Reaction equation

HRID 1663126 reaction equation
O[N:2]1C(=O)C2=CC=CC=C2C1=O.[CH:13]1([CH2:18][CH2:19][CH2:20][OH:21])[CH2:17][CH2:16][CH2:15][CH2:14]1>>[CH:13]1([CH2:18][CH2:19][CH2:20][O:21][NH2:2])[CH2:17][CH2:16][CH2:15][CH2:14]1

Participants

3

Reactant 2

HCID 10665N-HydroxyphthalimideHCID 69842Cyclopentanepropanol

Product 1

HCID 58989982O-(3-cyclopentylpropyl)hydroxylamine

Procedure

Prepared by a similar procedure as described for preparation 31. Starting materials: N-hydroxyphthalimide and 3-cyclopentyl-1-propanol (Aldrich). 13C-NMR (CDCl3) δ 76.5, 40.0, 32.7, 32.4, 27.7, 25.2.

Workup

  1. customPrepared by a similar procedure
  2. customas described for preparation 31

Sources & evidence

ORD record
ord-21d2fccdd8ae483ca7ee3e21c6d802ca
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

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