N-Hydroxyphthalimide → HCID 178514654, compound

HRID 1663127Notes

Reaction equation

HRID 1663127 reaction equation
O[N:2]1C(=O)C2=CC=CC=C2C1=O.[C@H:13]1([CH2:21][OH:22])[CH2:18][CH2:17][C@H:16]([CH2:19][OH:20])[CH2:15][CH2:14]1>>[NH2:2][O:20][CH2:19][C@H:16]1[CH2:17][CH2:18][C@H:13]([CH2:21][OH:22])[CH2:14][CH2:15]1

Participants

3

Reactant 2

HCID 10665N-HydroxyphthalimideHCID 178520956HCID 178520956, compound

Product 1

HCID 178514654HCID 178514654, compound

Procedure

Prepared by a similar procedure as described for preparation 31. Starting materials: N-hydroxyphthalimide and trans-1,4-cyclohexanedimethanol (Acros). 13C-NMR (CDCl3) δ 81.6, 68.2, 40.3, 36.8, 29.0, 28.7.

Workup

  1. customPrepared by a similar procedure
  2. customas described for preparation 31

Sources & evidence

ORD record
ord-4864f1bd1be9441e8ba42997514a27b7
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

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