HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine, hydrochloride (1:1) → HCID 58989882, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine, hydrochloride (1:1) | HCID 197884 | — |
| Reactant | HCID 58989917 | HCID 58989917 | — |
| Product | HCID 58989882 | HCID 58989882 | — |
Reaction Steps
Prepared by a similar procedure as described for preparation of example 405. Starting materials: 3-{2-[(Pyridin-4-ylmethyl)-amino]-benzoylaminooxymethyl}-benzoic acid (see example 403) and morpholine hydrochloride. 1H-NMR (DMSO-d6) δ 11.6 (bs, 1H), 8.49 (m, 2H), 7.89 (bt, 1H), 7.56 (m, 1H), 7.52-7.44 (m, 2H), 7.42-7.34 (m, 2H), 7.31 (m, 2H), 7.19 (m, 1H), 6.58-6.49 (m, 2H), 4.98 (s, 2H), 4.47 (d, 2H), 3.80-3.10 (m, 8H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08034811B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-b040d87c574a4dd69f7990b4ab5444a9 |
| Source note | uspto-grants-2011_10 |