1-(4-Pyridyl)piperazine → HCID 67435829, compound

HRID 1663239Notes

Reaction equation

HRID 1663239 reaction equation
[N:1]1[CH:6]=[CH:5][C:4]([N:7]2[CH2:12][CH2:11][NH:10][CH2:9][CH2:8]2)=[CH:3][CH:2]=1.Br[CH:14]([CH3:27])[CH2:15][N:16]1[C:20](=[O:21])[C:19]2=[CH:22][CH:23]=[CH:24][CH:25]=[C:18]2[C:17]1=[O:26]>>[N:1]1[CH:6]=[CH:5][C:4]([N:7]2[CH2:8][CH2:9][N:10]([CH:14]([CH3:27])[CH2:15][N:16]3[C:17](=[O:26])[C:18]4[C:19](=[CH:22][CH:23]=[CH:24][CH:25]=4)[C:20]3=[O:21])[CH2:11][CH2:12]2)=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 705171-(4-Pyridyl)piperazineHCID 594721HCID 594721, compound

Product 1

HCID 67435829HCID 67435829, compound

Procedure

The title compound was prepared from 1-pyridin-4-yl-piperazine [Org. Lett. 4 (2002) 737-740] and N-(2-bromopropyl)-phthalimide according to the method described in Reference Example 1/a.

Sources & evidence

ORD record
ord-e98f0973916a4eee85d1689072afc006
Source dataset
uspto-grants-2011_10
Patent number
US08034827B2

Reaction notes

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