HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → 3-Bromo-4-hydroxy-5-nitrobenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | 3-Bromo-4-hydroxybenzaldehyde | HCID 76308 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 3-Bromo-4-hydroxy-5-nitrobenzaldehyde | HCID 1494378 | — |
Reaction Steps
To a cooled solution of 3-bromo-4-hydroxybenzaldehyde (5 g) in acetic acid (50 ml) was added nitric acid (1.17 ml). The mixture was allowed to reach room temperature. After stirring for 17 h, the resulting precipitate was filtered off. The solid was washed with water and dried in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08034945B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-7621a148482142bf87e49eebabbd5208 |
| Source note | uspto-grants-2011_10 |