HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Naphthyl isopropyl ketone → alpha-Bromoisopropyl 2-naphthyl ketone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Naphthyl isopropyl ketone | HCID 10965495 | — |
| Reactant | Phenyltrimethylammonium bromide dibromide | HCID 17977687 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | alpha-Bromoisopropyl 2-naphthyl ketone | HCID 12587407 | 172.2% |
Reaction Steps
2.16 g of phenyltrimethylammonium tribromide was added to a mixture comprising 1.14 g of 2-naphthyl isopropyl ketone and 25 ml of tetrahydrofuran, and the mixture was reacted at room temperature for 3 hours. The reaction mixture was filtered, and the filtrate was concentrated under reduced pressure to obtain 1.59 g of oily α-bromoisopropyl 2-naphthyl ketone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08039420B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-8037e13c8f1c4a26a0fd6316a351b37f |
| Source note | uspto-grants-2011_10 |