Hydroxylamine → HCID 178513392, compound

Participants

Reaction Steps

Reaction of 4-((2-chloroethoxy)methyl)tetrahydro-2H-pyran-4-carbonitrile (10.78 g, 52.9 mmol) with hydroxylamine gave 10.59 g (84% yield) of the title material as a white solid. 1HNMR 400 MHz (CDCl3) δ (ppm): 1.60 (2H, m, CH2), 2.04 (2H, m, CH2), 3.52 (2H, s, CH2), 3.55-3.85 (8H, m, 4×CH2), 5.01 (2H, broad s). MS (ESI+) m/e 237 [M+H+].

Provenance & Evidence