HRID1664224

反应详情

EQUATION

反应方程式

HRID 1664224 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To the solution of 2.19 g (8.75 mmol) 3-nitro-5-(2-oxo-pyrrolidin-1-yl)-benzoic acid in 50 ml MeOH/THF 3/2 are added 0.2 g Pd/C (10% Engelhard 4505) and the reaction is stirred at rt under hydrogen (1 atm) for 18 h. After filtration through celite the solvent is evaporated at reduced pressure to give the product.

WORKUP

后处理

  1. filtrationAfter filtration through celite the solvent
  2. customis evaporated at reduced pressure
  3. customto give the product