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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1664511Generated: October 29, 2026

Hydrazine → HCID 178446164, compound

https://huagongshe.com/reaction/1664511

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrazineHCID 9321—
Reactant3-Pentyl-2-thioxo-1,2,3,7-tetrahydro-6H-purin-6-oneHCID 57600236—
SolventWaterHCID 962—
ProductHCID 178446164HCID 17844616479.4%

Reaction Conditions

Temperature100 °C

Reaction Steps

3-Pentyl-2-thioxo-1,2,3,7-tetrahydro-6H-purin-6-one (6.0 g, 16 mmol) was mixed with hydrazine (10 mL, 300 mmol) and water (10 mL). The mixture was heated at 100° C. for 8 h. The solid formed was filtered and washed with water to give the desired product (3.0 g, 78%). LCMS calculated for C10H17N6O (M+H): 237.1. found: 237.1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08039478B2
Source datasetuspto-grants-2011_10
ORD IDord-b0ccd06793cd451cbb2c6afb4e10dbb9
Source noteuspto-grants-2011_10