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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1664540Generated: October 29, 2026

Hydrazine → HCID 178446160, compound

https://huagongshe.com/reaction/1664540

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrazineHCID 9321—
Reactant8-cyclobutyl-3-pentyl-2-thioxo-1,2,3,7-tetrahydro-6H-purin-6-oneHCID 57600241—
SolventWaterHCID 962—
ProductHCID 178446160HCID 17844616038.6%

Reaction Conditions

Temperature100 °C

Reaction Steps

The mixture of 8-cyclobutyl-3-pentyl-2-thioxo-1,2,3,7-tetrahydro-6H-purin-6-one (0.6 g, 2.0 mmol) in 20 M of hydrazine in water (20 mL) was stirred at 100° C. overnight. After cooling to room temperature, the solid formed was filtered and dried Cooled down, the solid was isolated to give yield the desired product (230 mg, 38.6%). LCMS calculated for C14H23N6O (M+H): 291.2. found: 291.2.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08039478B2
Source datasetuspto-grants-2011_10
ORD IDord-396063735093497cbadbdcc54c57bac0
Source noteuspto-grants-2011_10