HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22975579, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67440963 | HCID 67440963 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 22975579 | HCID 22975579 | — |
Reaction Steps
Hydrochloric acid (4.0 N in dioxane; 4 mL, 16.0 mmol) was added to a solution of tert-butyl 4-oxo-1,3,8-triazaspiro[4.5]dec-1-ene-8-carboxylate (60 mg, 0.24 mmol) in dioxane (6 mL). After 18 h, the reaction mixture was concentrated to give the hydrochloride salt of the title compound. MS 154.1 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08039460B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-8c6739a2dfeb4380b37ed010b7100f62 |
| Source note | uspto-grants-2011_10 |