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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1664811Generated: November 2, 2026

Hydrochloric Acid → HCID 22975579, compound

https://huagongshe.com/reaction/1664811

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 67440963HCID 67440963—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 22975579HCID 22975579—

Reaction Steps

Hydrochloric acid (4.0 N in dioxane; 4 mL, 16.0 mmol) was added to a solution of tert-butyl 4-oxo-1,3,8-triazaspiro[4.5]dec-1-ene-8-carboxylate (60 mg, 0.24 mmol) in dioxane (6 mL). After 18 h, the reaction mixture was concentrated to give the hydrochloride salt of the title compound. MS 154.1 (M+1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08039460B2
Source datasetuspto-grants-2011_10
ORD IDord-8c6739a2dfeb4380b37ed010b7100f62
Source noteuspto-grants-2011_10