HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58032833, compound → HCID 66627249, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58032833 | HCID 58032833 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 66627249 | HCID 66627249 | — |
Reaction Steps
From 4-[(5-fluoro-thiophen-2-yl)-hydroxy-methyl]-piperidine-1-carboxylic acid tert-butyl ester (968 mg) by procedure E.2. MeCN (0.6 ml) was added to the reaction mixture. Yield: 577 mg (60%). Light brown gum. MS (m/z): 336.4 ([M+Na]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08039490B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-11207f7842f849a1be3d3dde3c1bad87 |
| Source note | uspto-grants-2011_10 |