Triethylamine → HCID 61410043, compound

HRID 1665074Notes

Reaction equation

HRID 1665074 reaction equation
Cl.[Br:2][C:3]1[CH:4]=[C:5]([CH:8]=[CH:9][CH:10]=1)[CH2:6][NH2:7].[CH:11]([S:14](Cl)(=[O:16])=[O:15])([CH3:13])[CH3:12].C(N(CC)CC)C>ClCCl>[Br:2][C:3]1[CH:4]=[C:5]([CH:8]=[CH:9][CH:10]=1)[CH2:6][NH:7][S:14]([CH:11]([CH3:13])[CH3:12])(=[O:16])=[O:15]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 824082-Propanesulfonyl chlorideHCID 27249803-Bromobenzylamine hydrochloride

Product 1

HCID 61410043HCID 61410043, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

In analogy to example 1, step 1, 3-bromobenzylamine hydrochloride was reacted with isopropylsulfonyl chloride and triethylamine in dichloromethane to give propane-2-sulfonic acid 3-bromo-benzylamide as a colorless solid. MS: 290.0 ([M−H]−)

Sources & evidence

ORD record
ord-2fe810d80d8441969e07492fc163d6f2
Source dataset
uspto-grants-2011_10
Patent number
US08039493B2

Reaction notes

Loading…