HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutyl iodide → HCID 25234317, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutyl iodide | HCID 10556 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | HCID 67438422 | HCID 67438422 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 25234317 | HCID 25234317 | — |
Reaction Steps
In analogy to example 10, step 3, propane-2-sulfonic acid (3′-methanesulfonyl-biphenyl-3-ylmethyl)-amide (example 49, step 2) was reacted with 1-iodo-2-methylpropane and cesium carbonate in N,N-dimethylacetamide to give propane-2-sulfonic acid isobutyl-(3′-methanesulfonyl-biphenyl-3-ylmethyl)-amide as an off-white solid. MS: 441.3 ([M+NH4]+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08039493B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-f82e80f5bc674b2d9286718bc7ba5228 |
| Source note | uspto-grants-2011_10 |