4-Chlorophenylacetyl chloride → HCID 57661841, compound

Participants

Reaction Steps

Compound 47 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, (4-chlorophenyl)acetyl chloride and conditions outlined in procedure N. M.p.=120-125° C.; 300 MHz 1H NMR (DMSO-d6) δ 7.91 (m, 2H), 7.74 (t, 1H), 7.56 (t, 1H), 7.35 (m, 2H), 7.25 (m, 2H), 4.10 (dd, 1H), 3.94 (m, 1H), 3.77 (dd, J=3.3 Hz, 2H), 3.57 (s, 2H), 3.09 (s, 2H), 2.05 (m, 2H), 1.67 (m, 2H); LCMS: 454 [M+H].

Provenance & Evidence