Benzoyl chloride, 3-chloro- → HCID 57662045, compound

Participants

Reaction Steps

Compound 62 was synthesized using spiro[azepane-4,2′-naphtho[1,2-b][1,4]oxathiine]-5′,6′-dione, 3-chlorobenzoyl chloride and conditions outlined in procedure N. M.p.=98-100° C., 400 MHz 1H NMR (CDCl3) δ: 8.08-8.06 (m, 1H), 7.76-7.66 (m, 2H), 7.52-7.48 (m, 1H), 7.42-7.21 (m, 4H), 3.87-3.86 (m, 1H), 3.67-3.49 (m, 3H), 3.05-2.92 (m, 2H), 2.39-2.17 (m, 4H), 2.04-1.96 (m, 1H), 1.89-1.76 (m, 1H); LCMS: 454 [M+H].

Provenance & Evidence