3-Chlorobenzenesulphonyl chloride → HCID 57662050, compound

Participants

Reaction Steps

Compound 82 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, 3-chlorobenzenesulfonyl chloride and conditions outlined in procedure P. M.p.=255-256° C.; 400 1H NMR (DMSO-d6) δ: 7.98-7.9 (m, 1H), 7.89-7.82 (m, 1H), 7.8-7.7 (m, 3H), 7.58-7.4 (m, 2H), 7.3 (d, J=7.6 Hz, 1H), 3.65-3.58 (m, 2H), 3.1 (s, 2H), 2.6-2.5 (m, 2H), 2.15-2.05 (m, 2H), 1.95-1.84 (m, 2H) LCMS: 476 [M+H].

Provenance & Evidence