HCID 53973062, compound → HCID 57661863, compound

Participants

Reaction Steps

Compound 151 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione and 1-fluoro-4-(3-iodopropoxy)benzene and conditions outlined in procedure V. M.p.=164-165° C.; 400 MHz 1H NMR (DMSO-d6) δ: 7.92-7.87 (m, 1H), 7.82-7.76 (m, 2H), 7.6-7.52 (m, 1H), 7.18-7.06 (m, 2H), 6.97-6.9 (m, 2H), 4.03-3.95 (m, 2H), 3.07 (s, 2H), 2.82-2.72 (m, 2H), 2.55-2.48 (m, 2H), 2.4-2.25 (m, 2H), 2.05-1.75 (m, 6H); LCMS: 454 [M+H].

Provenance & Evidence