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HRID1665363

反应详情

EQUATION

反应方程式

HRID 1665363 的结构方程式

REACTANTS

反应物

2
结构：C1CN(CC2CO2)CCO1
HCID97751

Morpholine, 4-(2-oxiranylmethyl)-

C7H13NO2

结构：O=C1C(=O)c2ccccc2C2=C1SCC1(CCNCC1)O2
HCID57661820

Spiro[naphtho[1,2-b]-1,4-oxathiin-2(3H),4′-piperidine]-5,6-dione

C16H15NO3S

PRODUCTS

生成物

1
结构：O=C1C(=O)c2ccccc2C2=C1SCC1(CCN(CC(O)CN3CCOCC3)CC1)O2
HCID57661892

未命名化合物

PROCEDURE

实验过程

Compound 166 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, 4-(oxiran-2-ylmethyl)morpholine and conditions outlined in procedure X. M.P.=75-78° C.; 400 MHz 1H NMR (CDCl3) δ: 8.05 (d, 1H), 7.75 (d, 1H), 7.65 (t, 1H), 7.5 (t, 1H), 3.9 (m, 1H), 3.7 (m, 5H), 2.95 (s, 1H), 2.9 (t, 2H), 2.7-2.3 (m, 11H), 2.15 (d, 2H), 1.9 (q, 2H); LCMS: 445 [M+H].