o-CRESYL GLYCIDYL ETHER → HCID 57661989, compound

HRID 1665370Notes

Reaction equation

HRID 1665370 reaction equation
[NH:1]1[CH2:6][CH2:5][C:4]2([O:11][C:10]3[C:12]4[C:17]([C:18](=[O:21])[C:19](=[O:20])[C:9]=3[S:8][CH2:7]2)=[CH:16][CH:15]=[CH:14][CH:13]=4)[CH2:3][CH2:2]1.[CH3:22][C:23]1[CH:33]=[CH:32][CH:31]=[CH:30][C:24]=1[O:25][CH2:26][CH:27]1[CH2:29][O:28]1>>[OH:28][CH:27]([CH2:26][O:25][C:24]1[CH:30]=[CH:31][CH:32]=[CH:33][C:23]=1[CH3:22])[CH2:29][N:1]1[CH2:2][CH2:3][C:4]2([O:11][C:10]3[C:12]4[C:17]([C:18](=[O:21])[C:19](=[O:20])[C:9]=3[S:8][CH2:7]2)=[CH:16][CH:15]=[CH:14][CH:13]=4)[CH2:5][CH2:6]1

Participants

3

Reactant 2

HCID 16640o-CRESYL GLYCIDYL ETHERHCID 57661820Spiro[naphtho[1,2-b][1,4]oxathiine-2,4'-piperidine]-5,6-dione

Product 1

HCID 57661989HCID 57661989, compound

Procedure

Compound 173 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, 2-[(2-methylphenoxy)methyl]oxirane and conditions outlined in procedure X. LCMS: 466 [M+H]; Rt=1.05 min.

Sources & evidence

ORD record
ord-4f883566058f458ea8a4d54ecfa0d93a
Source dataset
uspto-grants-2011_10
Patent number
US08039503B2

Reaction notes

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