129098-61-9 → HCID 57661967, compound

Participants

Reaction Steps

Compound 221 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, (2S)-2-[(2-naphthyloxy)methyl]oxirane and conditions outlined in procedure Y. M.p.=164-167° C., (DMSO-d6) δ: 7.91-7.87 (m, 1H), 7.84-7.78 (m, 5H), 7.6-7.52 (m, 1H), 7.48-7.4 (m, 1H), 7.38-7.3 (m, 2H), 7.2-7.14 (m, 1H), 5.0-4.93 (m, 1H), 4.2-3.97 (m, 3H), 3.07 (s, 2H), 2.93-2.76 (m, 2H), 2.63-2.4 (m, 4H), 2.06-1.93 (m, 2H), 1.9-1.78 (m, 2H); LCMS=502 [M+H].

Provenance & Evidence