HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminobiphenyl → Formamide, N-(1,1'-biphenyl)-4-yl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminobiphenyl | HCID 7102 | — |
| Reactant | Ethyl formate | HCID 8025 | — |
| Product | Formamide, N-(1,1'-biphenyl)-4-yl- | HCID 95684 | 86.2% |
Reaction Steps
A mixture of biphenyl-4-ylamine (100 mg, 0.59 mmol) and ethylformate (1 mL) was stirred at reflux temperature for 1 hr. After the completion of the reaction, the reaction mixture was quenched with cold water. The precipitate was filtered to afford 100 mg (86.2% Yield) of N-biphenyl-4-yl-formamide as the required product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08039463B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-830b7b86db6041399a8280fc346fdbba |
| Source note | uspto-grants-2011_10 |