HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoropyridine → HCID 24947346, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoropyridine | HCID 9746 | — |
| Reactant | 3,4-Difluoroaniline | HCID 77469 | — |
| Reactant | 4-(Bromomethyl)-1,2-difluorobenzene | HCID 581436 | — |
| Product | HCID 24947346 | HCID 24947346 | — |
Reaction Steps
The title compound was prepared in four steps from 3,4-difluoroaniline, 2-fluoropyridine and 3,4-difluorobenzyl bromide as described in Procedure B. The crude product was purified by preparative LC-MS to give the title compound as the free base (yellowish solid). MS (ES+) m/z 333 ([M+1]+, 100); HR-MS: 333.1008 ([M+1]+, C18H13F4N2; calc. 333.101485).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08039632B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-e2b96e7b50f847fba8ce9ad51fce2da6 |
| Source note | uspto-grants-2011_10 |