HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Fluoro-2-methylbenzenesulphonyl chloride → HCID 67442564, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Fluoro-2-methylbenzenesulphonyl chloride | HCID 136286 | — |
| Reactant | HCID 44224963 | HCID 44224963 | — |
| Product | HCID 67442564 | HCID 67442564 | 88% |
Reaction Steps
According to general sulfonamide coupling procedure, [5-(4-Chloro-phenyl)-1-(2,4-dichloro-phenyl)-4,5-dihydro-1H-pyrazole-3-yl]methyl amine hydrochloride was reacted with 5-fluoro-2-methylbenzenesulfonyl chloride. The reaction yield was 88% of 2-Chloro-N-[5-(4-Chloro-phenyl)-1-(2,4-dichloro-phenyl)-4,5-dihydro-1H-pyrazole-3-ylmethyl]-5-fluoro-2-methyl-benzenesulfonamide as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08044053B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-ed8c4265ee2046b7974fca89811d0754 |
| Source note | uspto-grants-2011_10 |