HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbonic acid, bis(1,1-dimethylethyl) ester → HCID 12189552, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbonic acid, bis(1,1-dimethylethyl) ester | HCID 10219638 | — |
| Reactant | HCID 15175833 | HCID 15175833 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 12189552 | HCID 12189552 | — |
Reaction Steps
The compound obtained in Step (ii) was subjected to reduction with lithium aluminum hydride in THF. Then, the resultant was subjected to Boc-introducing reaction with di-tert-butyl carbonate to give the subtitle compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08044056B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-9d9b8ce6807f44dfbbc024f9aa6f9fe5 |
| Source note | uspto-grants-2011_10 |