HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxybenzaldehyde → HCID 2692519, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxybenzaldehyde | HCID 11569 | — |
| Reactant | tert-Butyl carbazate | HCID 70091 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 2692519 | HCID 2692519 | 103.1% |
Reaction Steps
A solution of 3-methoxybenzaldehyde (27.0 g) and t-butyl carbazate (25.0 g) in tetrahydrofuran (350 ml) was refluxed for 4 hours. The reaction mixture was concentrated to dryness giving t-butyl 3-methoxybenzylidenecarbazate (48.8 g) as an oil, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08044067B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-d3c6225cf04a482db931a1cbf557ef49 |
| Source note | uspto-grants-2011_10 |