Sodium Hydroxide → HCID 20240767, compound

Participants

Reaction Steps

The solution of 0.2 g (0.9 mmol) ethyl-(1,3-benzoxazol-2-yloxy)acetate and 0.4 g (1 mmol) sodium hydroxide in 1 ml water is stirred for 2 hours at room temperature, then extracted with 3×5 ml chloroform. The united organic phase is dried over sodium sulfate and evaporated in vacuum to obtain 54 mg title compound as an oil. LC-MS[MH+]=194 (C9H7NO4 193.16)

Provenance & Evidence