HRID1666822
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
产物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Add 6-trifluoromethyltryptamine to 1:1 acetone/Et2O. Add dropwise of oxalic acid (1.2 eq.) in acetone to give a solid. Collect the solid by filtration and dry overnight in the vacuum oven to obtain the title compound: MS (ES+): m/z 212 (M−NH2)+; (ES−): m/z 227 (M−H)−.
WORKUP
后处理
- customto give a solid
- customCollect the solid
- filtrationby filtration
- customdry overnight in the vacuum oven