HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic Acid → HCID 21071614, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic Acid | HCID 971 | — |
| Reactant | HCID 18317967 | HCID 18317967 | — |
| Reactant | Acetone diethylether | HCID 21584533 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 21071614 | HCID 21071614 | — |
Reaction Steps
Add 6-trifluoromethyltryptamine to 1:1 acetone/Et2O. Add dropwise of oxalic acid (1.2 eq.) in acetone to give a solid. Collect the solid by filtration and dry overnight in the vacuum oven to obtain the title compound: MS (ES+): m/z 212 (M−NH2)+; (ES−): m/z 227 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08044090B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-aa2e92ef5cb240b894f4d812a5011db8 |
| Source note | uspto-grants-2011_10 |