Hydrochloric Acid → HCID 67358282, compound

Participants

Reaction Steps

The product from Example 44A (0.071 g, 0.198 mmol) was added to HCl (2.0 Min dioxane) (0.991 mL, 1.981 mmol), and methanol was added dropwise until the reaction became nearly homogeneous. As the reaction was stirred, a precipitate formed. The reaction was concentrated to give the title compound (0.066 g, 0.256 mmol) as the dihydrochloride salt. MS (APCI) m/z 259 (M+H)+.

Provenance & Evidence