Hydrochloric Acid → HCID 67358827, compound

Participants

Reaction Steps

To a solution of product from Example 180A (0.14 g) in methanol (5 mL) was added 4 N HCl in dioxane (1 mL), and the mixture was stirred at room temperature for 2 hours. The reaction mixture was concentrated to yield the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 8.81 (bs, 2H), 7.95 (m, 1H), 7.84 (m, 2H), 7.71 (t, J=7.73 Hz, 1H), 4.63 (s, 2H), 4.23 (m, 5H); MS (DCI) m/z 231 (M+H)+.

Provenance & Evidence