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HRID1667306

反应详情

EQUATION

反应方程式

HRID 1667306 的结构方程式

REACTANTS

反应物

4
结构：CCO
HCID702

Ethanol

C2H6O

结构：[C-]#[N+]CS(=O)(=O)c1ccc(C)cc1
HCID161915

Tosylmethyl isocyanide

C9H9NO2S

结构：CC(C)(C)OC(=O)N1C2CCC1CC(=O)C2
HCID2794767

tert-Butyl 3-oxo-8-azabicyclo[3.2.1]octane-8-carboxylate

C12H19NO3

结构：CC(C)(C)[O-].[K+]
HCID23665647

2-Methyl-2-propanol, potassium salt

C4H9KO

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1C2CCC1CC(C#N)C2
HCID53487658

tert-Butyl 3-cyano-8-azabicyclo[3.2.1]octane-8-carboxylate

C13H20N2O2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：COCCOC
溶剂HCID8071

未命名化合物

PROCEDURE

实验过程

tert-Butyl 3-oxo-8-azabicyclo[3.2.1]octane-8-carboxylate was reacted in the presence of p-toluenesulfonylmethylisocyanide, potassium tert-butoxide and ethanol in 1,2-dimethoxyethane to produce tert-butyl 3-cyano-8-azabicyclo[3.2.1]octane-8-carboxylate.