HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67417031, compound → HCID 67417025, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67417031 | HCID 67417031 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 67417025 | HCID 67417025 | — |
Reaction Steps
A solution of (4-chloro-3′-hydroxy-biphenyl-3-yl)-carbamic acid tert-butyl ester (1.8 g, 5.64 mmol) was dissolved in a solution of HCl in i-PrOH (5-6M, 20 mL). The resulting solution was stirred at RT for 6 hrs then concentrated to provided 3′-amino-4′-chloro-biphenyl-3-ol hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08044041B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-08d9ad8b79cf416b841165e32fb4bf37 |
| Source note | uspto-grants-2011_10 |