HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67444123, compound → HCID 57448187, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67444123 | HCID 67444123 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 57448187 | HCID 57448187 | 110% |
Reaction Steps
6F (130 mg, 0.29 mmol) was dissolved in THF (8 mL). To this solution was added 10% Pd/C (cat.), and the mixture was hydrogenated at 50 psi for 16 h. The reaction was filtered and concentrated to provide 6G (113 mg, 10%). LC-MS: 355.19 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08044242B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-c273d2cbc2a142a7858d75cc81f15fbe |
| Source note | uspto-grants-2011_10 |