HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67443655, compound → HCID 67446119, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67443655 | HCID 67443655 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 67446119 | HCID 67446119 | — |
Reaction Steps
A mixture of 13B (85 mg, 0.15 mmol) and Pd/C (cat.) was hydrogenated at 40 psi overnight. The reaction was filtered and concentrated to provide 13C (39 mg, 99%). LC-MS: 482.37 (M+Na)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08044242B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-274d211d12ae4e7cb81b177c0650c59a |
| Source note | uspto-grants-2011_10 |