Acetyl chloride → HCID 59239869, compound

Participants

Reaction Steps

A mixture of the compound (50 mg) obtained in Example 13, acetyl chloride (10 mg), triethylamine (18 mg) and tetrahydrofuran (1 ml) was stirred at room temperature for 30 min. The reaction mixture was diluted with ethyl acetate and water, and the precipitate was collected by filtration to give the title compound (39 mg) as a colorless powder.

Provenance & Evidence