HRID1668404

反应详情

EQUATION

反应方程式

HRID 1668404 的结构方程式

PROCEDURE

实验过程

A mixture of the compound (0.92 g) obtained in Example 29 and 4N hydrogen chloride-ethyl acetate solution was stirred at room temperature for 3 hr. The solvent was evaporated under reduced pressure, and the residue was washed with ethyl acetate to give the title compound (115 mg) as a colorless powder.

WORKUP

后处理

  1. customThe solvent was evaporated under reduced pressure
  2. washthe residue was washed with ethyl acetate