HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66995204, compound → HCID 15985678, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66995204 | HCID 66995204 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15985678 | HCID 15985678 | 12% |
Reaction Steps
Compound 20D (55 mg, 0.094 mmol) in ethanol (2 mL) is hydrogenated under 10% palladium on carbon (10 mg) and hydrogen (balloon pressure). The reaction is monitored by LCMS. Upon completion the mixture is filtered and the filtrate is concentrated and purified by HPLC to afford the title compound (5 mg, 12%):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07989441B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-7fa204221c0a4a7b8690558fc2c6e12f |
| Source note | uspto-grants-2011_08 |