Sodium Carbonate → HCID 59150471, compound

Participants

Reaction Steps

Treatment of 3-ethyl-7-(trifluoroacetyl)-6,7,8,9-tetrahydro-5H-isoxazolo[4,5-h][3]benzazepine (21 mg) with Na2CO3 (1 mL, 1 M in water) in MeOH (2 mL) at reflux for 3 h followed by partitioning between water and dichloromethane and evaporation of the volatiles from the organic phase gave the title compound as a solidifying yellow oil in quantitative yield. The material was used as such without further characterisation.

Provenance & Evidence