HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 59150525, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 59150524 | HCID 59150524 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 59150525 | HCID 59150525 | 62% |
Reaction Steps
A solution of N-(2,2-dimethoxy-ethyl)-2-(3-methoxy-2-methyl-phenyl)-acetamide (23 g) in a mixture of acetic acid (40 ml) and conc. HCl (40 ml) was stirred at room temperature for 24 hours. Ice was added with vigorous stirring and the obtained precipitated was filtered (10.9 g, 62% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07989444B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-74ac2c9c7c264d6cb6fc736daf790d28 |
| Source note | uspto-grants-2011_08 |