HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 67359067, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 67359454 | HCID 67359454 | — |
| Product | HCID 67359067 | HCID 67359067 | — |
Reaction Steps
7-Methoxy-6-methyl-2,3,4,5-tetrahydro-1H-benzo[d]azepine hydrochloride (8.6 g) was treated with 48% HBr (100 ml) at 110° C. for 4 hours; volatiles were evaporated under reduced pressure obtaining crude 7-hydroxy-6-methyl-1,2,4,5-tetrahydro-3H-3-benzazepine hydrobromide (10.2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07989444B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-9a2420a9088c4799bbc0cba224b66622 |
| Source note | uspto-grants-2011_08 |