HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 57825114, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 19048532 | HCID 19048532 | — |
| Product | HCID 57825114 | HCID 57825114 | 86% |
Reaction Steps
In analogy to the procedure described for Building Block AW, the alkylation of 2-(3,5-dibromo-phenyl)-ethanol with iodomethane using sodium hydride as the base yielded the title compound 86% yield as a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07989449B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-91eb8c64fa804e969008394faa25e362 |
| Source note | uspto-grants-2011_08 |