HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 67344786, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 67345302 | HCID 67345302 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67344786 | HCID 67344786 | — |
Reaction Steps
A solution of (7R)-7-[(2-{3-[{[(tert-butoxycarbonyl)amino]sulfonyl}(methyl)amino]pyrrolidin-1-yl}ethyl)(methyl)amino]-14-cyclohexyl-7,8-dihydro-6H-indolo[1,2-e][1,5]benzoxazocine-11-carboxylic acid in DCM was treated with TFA and the solution was left stirring for 1 h. All volatiles were removed in vacuo to leave the product as pale yellow foam. (ES+) m/z 610 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07989438B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-11204653d5954c02b52d97663b792e9c |
| Source note | uspto-grants-2011_08 |