Hydrochloric Acid → HCID 23729141, compound

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Reaction Steps

To the carboxylic acid from step 2 (65 mg) was added 4.0 M HCl in dioxane (1.0 mL). After 3 h, the dioxane was removed to give 58 mg of product. 1H NMR (400 MHz, DMSO-d6) δ 3.11-3.28 (m, 2H), 4.20 (t, J=6.0 Hz, 1H), 6.94-7.15 (m, 9H), 7.27-7.32 (m, 2H), 7.36-7.42 (m, 2H); LCMS; 99%, ESI−, Calcd: 349.39 m/z. Found 348.5 (M−1) m/z.

Provenance & Evidence