HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzamide → HCID 178437757, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzamide | HCID 2331 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 2-Amino-4-methoxy-3-methylbenzamide | HCID 59165435 | — |
| Product | HCID 178437757 | HCID 178437757 | 100% |
Reaction Steps
The general procedure described in Example 31 was followed using 2-amino-4-methoxy-3-methyl benzamide as benzamide derivative [A] and acetic acid chloride as acid chloride [B], which gave the title compound (2.2 g, 100%). 1H-NMR DMSO-D6 δ 1.2 (m, 3H), 2.38 (s, 3H), 2.6 (m, 2H), 3.90 (s, 3H), 7.18 (d, 2H), 7.96 (d, 2H), 11.88 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07989471B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-4ec9c1eab3d54b5e90f6c2fc3bc1f6d5 |
| Source note | uspto-grants-2011_08 |