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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1669589Generated: November 1, 2026

Benzamide → HCID 178437757, compound

https://huagongshe.com/reaction/1669589

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzamideHCID 2331—
ReactantAcetyl chlorideHCID 6367—
Reactant2-Amino-4-methoxy-3-methylbenzamideHCID 59165435—
ProductHCID 178437757HCID 178437757100%

Reaction Steps

The general procedure described in Example 31 was followed using 2-amino-4-methoxy-3-methyl benzamide as benzamide derivative [A] and acetic acid chloride as acid chloride [B], which gave the title compound (2.2 g, 100%). 1H-NMR DMSO-D6 δ 1.2 (m, 3H), 2.38 (s, 3H), 2.6 (m, 2H), 3.90 (s, 3H), 7.18 (d, 2H), 7.96 (d, 2H), 11.88 (s, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07989471B2
Source datasetuspto-grants-2011_08
ORD IDord-4ec9c1eab3d54b5e90f6c2fc3bc1f6d5
Source noteuspto-grants-2011_08