HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67334113, compound → HCID 44199384, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67334113 | HCID 67334113 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 44199384 | HCID 44199384 | — |
Reaction Steps
(2-Methoxy-benzyl)-(5-nitro-quinolin-2-yl)-amine (2.2 g, 7.1 mmol) was dissolved in 100 mL methanol. Palladium on charcoal (10%, 150 mg, 0.14 mmol) was added and the reaction mixture war hydrogenated with a hydrogen balloon overnight. The palladium was filtered off and the solvent was evaporated. The title compound was obtained as a yellow solid (1.98 g, 100%), MS: m/e=280.4 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07989628B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-88d3953fab994a00a4f826e2e56d8d9b |
| Source note | uspto-grants-2011_08 |