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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1669697Generated: October 29, 2026

HCID 67334113, compound → HCID 44199384, compound

https://huagongshe.com/reaction/1669697

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67334113HCID 67334113—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 44199384HCID 44199384—

Reaction Steps

(2-Methoxy-benzyl)-(5-nitro-quinolin-2-yl)-amine (2.2 g, 7.1 mmol) was dissolved in 100 mL methanol. Palladium on charcoal (10%, 150 mg, 0.14 mmol) was added and the reaction mixture war hydrogenated with a hydrogen balloon overnight. The palladium was filtered off and the solvent was evaporated. The title compound was obtained as a yellow solid (1.98 g, 100%), MS: m/e=280.4 (M+H+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07989628B2
Source datasetuspto-grants-2011_08
ORD IDord-88d3953fab994a00a4f826e2e56d8d9b
Source noteuspto-grants-2011_08