HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57438911, compound → HCID 67343450, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57438911 | HCID 57438911 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67343450 | HCID 67343450 | — |
Reaction Steps
3-Methyl-5-[4-(tert-butyl)phenyl]isoxazole (900 mg, 4.18 mmol) is introduced into 20 ml of ethanol, platinum(IV) oxide catalyst (90 mg) is added and the mixture is then hydrogenated under atmospheric pressure hydrogen for 12 h. The catalyst is filtered off and the filtrate is concentrated. 897 mg (99% of theory) of the title compound are obtained as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07989633B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-3ce0f9780f3b43fd84b9e37f584c244c |
| Source note | uspto-grants-2011_08 |