HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-methylbutane → Isopentadecan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-methylbutane | HCID 7891 | — |
| Reactant | 1-Decanol, 10-bromo- | HCID 104507 | — |
| Product | Isopentadecan-1-ol | HCID 94094 | 62% |
Reaction Steps
13-methyltetradecan-1-ol was prepared from 10-bromodecanol and 3-methylbutylbromide in 62% yield. The 1H NMR and MS-ESI data matched those reported by Yuasa et al. (Yuasa and Tsuruta (2004) Flavour and Fragrance Journal 19:199-204).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07994143B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-739e74c236e94a4c8d44ebfd30a74ead |
| Source note | uspto-grants-2011_08 |